Nuclear Magnetic Resonance Facility

Alex Greenwood

The NMR facility in the Chemistry department currently houses three solution NMR instruments ranging from 400-500 MHz. These include two walk-up Bruker 400s (an AVANCE NEO and an AVANCE I) with Z-Grad BBFO (Z-Gradient Broadband and Fluorine Observe) ATM (Automatic Tune and Match) probes and SampleXpress Lite automatic sample changers, and a Bruker DMX-500 with Z-Grad triple and double resonance probes. The NMR facility is capable of proton, carbon-13 and other multi-nuclear NMR in one, two, and three dimensions. Common experiments include HSQC (Heteronuclear Single-Quantum Coherence), COSY (COrrelated SpectroscopY), NOESY (Nuclear Overhauser Enhancement SpectroscopY), and DOSY (Diffusion-Ordered SpectroscopY). 
 
Location & Hours:
The Chemistry NMR facility is located in Crosley Tower, rooms 123 and 108. Walk-up instruments are available 24/7 for trained users.

Services32
  • SENSORS Nicolet FTIR spectrometer & microscope unassisted

    Cost:

    $40.00/hr

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  • SENSORS (ESEM) Environmental Scanning Electron Microscope assisted

    Cost:

    $90.00/hr

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  • SENSORS INSTRUMENTS GROUP 1 UNASSISTED (see instruments below)

    Cost:

    $10.00/hr

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  • SENSORS Veeco multimode scanning probe microscope

    Cost:

    $40.00/hr

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  • SENSORS INSTRUMENTS GROUP 2 UNASSISTED (see instruments below)

    Cost:

    $30.00/hr

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  • X-Ray Data Set Academic/SAMPLE

    Cost:

    $100.00/hr

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  • X-Ray Setup Academic/SAMPLE

    Cost:

    $15.00/hr

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  • X-Ray Unit Cell Only Academic/SAMPLE

    Cost:

    $50.00/hr

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  • X-ray synchtron /SAMPLE (formerly Beamline consortium time/SAMPLE)

    Cost:

    $50.00/hr

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  • NMR 500 1-8 HRS (1/2/ HR MINIMUM)/hour

    Cost:

    $8.00/hr

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  • NMR 500 9-24 HRS/hour

    Cost:

    $6.00/hr

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  • NMR 500 >24 HRS/hour

    Cost:

    $4.00/hr

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  • NMR AV400, AMX400 1-8 HRS (1/2/ HR MINIMUM)/hour

    Cost:

    $6.00/hr

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  • NMR AV400, AMX400 9-24 HRS/hour

    Cost:

    $5.00/hr

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  • NMR AV400, AMX400 >24 HRS/hour

    Cost:

    $3.00/hr

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  • ICP-MS Academic Qualitative Analysis/hour

    Cost:

    $38.00/hr

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  • ICP-MS Academic Quantitative Analysis/hour

    Cost:

    $38.00/hr

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  • ICP-MS Academic Quantitative Setup fee/sample

    Cost:

    $50.00/hr

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  • ICP-MS Academic Qualitative Analysis Set Up Fee/sample

    Cost:

    $38.00/hr

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  • ICP-MS Academic Qualitative Sample Prep/hour

    Cost:

    $38.00/hr

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  • ICP-MS Academic Quantitative Analysis Sample Prep/hour

    Cost:

    $38.00/hr

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  • ICP-MS Academic QA Time Resolved Set Up fee/sample run

    Cost:

    $109.00/hr

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  • ICP-MS Academic QA Time Resolved/sample

    Cost:

    $38.00/hr

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  • ICP-MS Academic QA Time Resolved per hour/if cheaper than per sample

    Cost:

    $109.00/hr

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  • ICP-MS Academic QA Time Resolved Sample prep/hour

    Cost:

    $38.00/hr

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  • MASSSPEC General MS/hour

    Cost:

    $80.00/hr

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  • MASSSPEC MS ANALYSIS (<1000 Da) rate/sample

    Cost:

    $25.00/hr

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  • MASSSPEC MS ANALYSIS (>1000 Da) rate/sample

    Cost:

    $35.00/hr

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  • MASSSPEC GC-MS per injection

    Cost:

    $120.00/hr

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  • MASSSPEC LC-MS per injection

    Cost:

    $25.00/hr

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  • MASSSPEC GC-MS self operated/hour (1/2 hour minimun)

    Cost:

    $15.00/hr

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  • MASSSPEC LTQ-FTMS SURCHARGE/SAMPLE

    Cost:

    $2.00/hr

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Equipment0